The current volume continues the tradition of the Organic Syntheses series, providing carefully checked and edited experimental procedures that describe important synthetic methods, transformations, reagents, and synthetic building blocks or intermediates with demonstrated utility in organic synthesis. These significant and interesting procedures should prove worthwhile to many synthetic chemists working in increasingly diverse areas. A trusted guide for professionals in organic and medicinal chemistry in academia, government, and industries, including pharmaceuticals, fine chemicals, agrochemicals, and biotechnological products.
By:
Richmond Sarpong
Imprint: John Wiley & Sons Inc
Country of Publication: United States
Weight: 857g
ISBN: 9781394200863
ISBN 10: 1394200862
Series: Organic Syntheses
Pages: 448
Publication Date: 22 June 2023
Audience:
Professional and scholarly
,
Undergraduate
Replaced By: 9781394278121
Format: Hardback
Publisher's Status: Active
Chapter 1 Synthesis of [(R)-DTBM-SEGPHOS]NiCl2 for the Enantioselective Acetal Formation from N-Propanoyl-1,3-Thiazinane-2-thione and Trimethyl Orthoformate Chapter 2 Synthesis of Alkylboronic Esters from Alkyl Iodides Chapter 3 Preparation of N-Formylamides by Oxidative Cleavage of N-Acylaminoacids Chapter 4 Transition-Metal-Free Synthesis of an Aryl Boronate Ester through Base-Mediated Boryl Substitution of an Aryl Halide with a Silylborane Chapter 5 A Convenient Method for the Removal of Tetrabutylammonium Salts from Desilylation Reactions Chapter 6 Discussion Addendum for: Asymmetric Michael Reaction of Aldehydes and Nitroalkenes Chapter 7 Preparation of a Donor-Acceptor Stenhouse Adduct (DASA): 5-((2Z,4E)-5-(Diethylamino)-2-hydroxypenta-2,4-dien-1-ylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione Chapter 8 Preparation of MIDA Anhydride and Reaction with Boronic Acids Chapter 9 Discussion Addendum for: Preparation of 1,1-Difluoroallenes by Difluorovinylidenation of Carbonyl Compounds Chapter 10 Ethoxypillar[6]arene Chapter 11 Organocatalytic Dimerization of Succinaldehyde Chapter 12 Synthesis of Phenanthridinones via the Palladium-Catalyzed Annulation of Benzyne Chapter 13 Synthesis of Triphenylene via the Palladium–Catalyzed Annulation of Benzyne Chapter 14 Synthesis of (((1R,3S,3′S)-3,3′-Diethyl-3H,3′H-1,1′-spirobi[isobenzofuran]-7,7′-diyl)bis(oxy))bis(diphenylphosphane) Chapter 15 Discussion Addendum for: Nickel-Catalyzed Cross-Coupling of Aryl Halides with Alkyl Halides: Ethyl 4-(4-(4-methylphenylsulfonamido)-phenyl)butanoate Chapter 16 Discussion Addendum for: Detrifluoroacetylative Diazo Group Transfer: (E)-1-Diazo-4-phenyl-3-buten-2-one Chapter 17 Preparation of 9-Azabicyclo[3.3.1]nonane-N-oxyl (ABNO) Chapter 18 Discussion Addendum for: Synthesis of N-Boc-N-Hydroxymethyl-L-phenylalaninal and Methyl trans-Oxazolidine-5-carboxylate, Chiral Synthons for threo-β-Amino-α-hydroxy Acids Chapter 19 Large Scale Oxidative Cyclization of (E)-Hex-3-en-1-yl(4-Methoxyphenyl)sulfamate Chapter 20 Synthesis of Carboxylic Acids from Benzamide Precursors Using Nickel Catalysis Chapter 21 Stereoselective Synthesis of Dimethyl 4(S)-Allyl-N-Boc-L-glutamate and Related Congeners Chapter 22 Discussion Addendum for: Preparation of Diisopropylammonium Bis(catecholato)cyclohexylsilicate Chapter 23 Preparation of 1,2:5,6-Di-O-cyclohexylidene-D-mannitol and 2,3-Cyclohexylidene-D-glyceraldehyde Chapter 24 Transformation of a N,N-Dimethylaniline N-oxide into a Tetrahydroquinoline Scaffold via a Formal Polonovski-Povarov Reaction Index
